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¹H AND 13C NMR SPECTRAL ASSIGNMENTS AND X-RAY CRYSTALLOGRAPHY OF 4,5,8,12b-TETRAHYDRO-ISOINDOLO[1,2 -α ]ISOQUINOLINE AND DERIVATIVES
Abstract
"12b-Hydroxy-5,6,8,12b-tetrahydroisoindolo[1,2-α] isoquinolin-8-one (4), 5,6,8,12b-tetrahydroisoindolo[1,2-α]isoquinoline (5) and 12b-hydroxy-5,6,8,12b-tetrahydroisoindolo[1,2-α]isoquinoline (6) were obtained by reduction of 4,5,8,12b-tetrahydroisoindolo[1,2-α]isoquinolin-8-one (3) with LiAlH4/THF/N2. The precursor and products were characterized by NMR spectroscopy and the X-ray crystal structure of 5 hydrochloride monohydrate (5a) was determined.
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| Título según SCIELO: | ¹H AND 13C NMR SPECTRAL ASSIGNMENTS AND X-RAY CRYSTALLOGRAPHY OF 4,5,8,12b-TETRAHYDRO-ISOINDOLO[1,2 -α ]ISOQUINOLINE AND DERIVATIVES |
| Título de la Revista: | JOURNAL OF THE CHILEAN CHEMICAL SOCIETY |
| Volumen: | 57 |
| Número: | 1 |
| Editorial: | 2013 |
| Fecha de publicación: | 2012 |
| Página de inicio: | 972 |
| Página final: | 976 |
| Idioma: | en |
| URL: | http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000100004&lng=en&nrm=iso&tlng=en |
| DOI: |
10.4067/S0717-97072012000100004 |
| Notas: | SCIELO |