Synthesis and Characterization of Chitosan –PHB Blends
Keywords: blends, chitosan, hydroxybutirate, deacetylation degree
Abstract
Blends of chitosan, [poly( ß-1,4)-2-amino-2-deoxy-D-glucopyranose], CH, the desacetylated product of chitin, with poly(3-hydroxybutyrate), PHB, usingratios of 90/10, 75/25, 50/50, 25/75, and 10/90 of chitosan-PHB were obtained. The blends were obtained using trifluoracetic acid as co-solvent under continue stirring at room temperature. Chitosan was obtained from shrimps shells of `Mv = 81,430 Daltons and 91% deacetylation degree, DS, was used. The PHB comes from biological fermentation process (Copersucar, Sao Paulo, Brazil) and their `Mv = 183,200 Daltons. The elastomeric products were characterized by elemental analyses, thermogravimetry, FT-IR and SEM.
Más información
Título de la Revista: | BOLETIN DE LA SOCIEDAD CHILENA DE QUIMICA |
Volumen: | 47 |
Número: | 4 |
Editorial: | Sociedad Chilena de Química |
Fecha de publicación: | 2002 |
Página de inicio: | 75 |
Página final: | 86 |
DOI: |
http://dx.doi.org/10.4067/S0366-16442002000400025 |
Notas: | ISI, http://dx.doi.org/10.4067/S0366-16442002000400025 |