Induction heating consolidation of TiO2 sol-gel coating on stainless steel support for photocatalysis applications

Dreidy Vásquez, Oscar Jerez, Rodrigo Schrebler, Carlos Carlesi, Danilo Carvajal, Nelson Cáceres, Ricardo Schrebler.

Keywords: Induction heating sintering, Electrochemical techniques, Coatings, Titanium dioxide, Photocatalysis, Azo dye

Abstract

A high-frequency induction heater was used to sinter titanium dioxide thin film on stainless steel plates with the aim of being used as photo-electrodes in wastewaters treatment. To validate the use of this sintering technique, the electrodes were pre-pared using sol-gel and dip-coating, followed by two different annealing processes for comparison: a conventional furnace and a high-frequency induction heating. To characterize the electrodes, X-ray diffraction (XRD), scanning electron micros-copy (SEM) and electrochemical and photocatalysis tests were performed. Anatase and rutile phases were obtained for both annealing techniques. A more regular surface morphology was achieved via the induction heating (IH) treatment at 300ºC. The impedance study showed a lower resistance of IH samples, representing an improvement in the charge carrier separation and its fast transfer to the surface of the electrode. The photo-oxidation of methylene blue exhibited a higher degradation compared with the conventional furnace samples prepared in this study

Más información

Título de la Revista: Periodica Polytechnica Chemical Engineering.
Volumen: 60
Número: 3
Editorial: BUDAPEST UNIV TECHNOLOGY ECONOMICS
Fecha de publicación: 2016
Página de inicio: 141
Página final: 151
Idioma: English
Notas: ISI