Induction heating consolidation of TiO2 sol-gel coating on stainless steel support for photocatalysis applications
Keywords: Induction heating sintering, Electrochemical techniques, Coatings, Titanium dioxide, Photocatalysis, Azo dye
Abstract
A high-frequency induction heater was used to sinter titanium dioxide thin film on stainless steel plates with the aim of being used as photo-electrodes in wastewaters treatment. To validate the use of this sintering technique, the electrodes were pre-pared using sol-gel and dip-coating, followed by two different annealing processes for comparison: a conventional furnace and a high-frequency induction heating. To characterize the electrodes, X-ray diffraction (XRD), scanning electron micros-copy (SEM) and electrochemical and photocatalysis tests were performed. Anatase and rutile phases were obtained for both annealing techniques. A more regular surface morphology was achieved via the induction heating (IH) treatment at 300ºC. The impedance study showed a lower resistance of IH samples, representing an improvement in the charge carrier separation and its fast transfer to the surface of the electrode. The photo-oxidation of methylene blue exhibited a higher degradation compared with the conventional furnace samples prepared in this study
Más información
Título de la Revista: | Periodica Polytechnica Chemical Engineering. |
Volumen: | 60 |
Número: | 3 |
Editorial: | BUDAPEST UNIV TECHNOLOGY ECONOMICS |
Fecha de publicación: | 2016 |
Página de inicio: | 141 |
Página final: | 151 |
Idioma: | English |
Notas: | ISI |