Abstract

This contribution describes an updated synthetic route along with full characterization of [{CpFe} 2-p-Ph’] with p-Ph’: p-Bis {2, 3, 4, 5-tetramethylcyclopentadienyl} benzene). The complex reported here was characterized by 1 H and 13 C NMR, elemental analysis, the X-ray crystal structure, and Mo? ssbauer spectroscopy. From the crystallographic analysis, it was found that both {CpFe} fragments are coordinated to opposite sites of the p-Ph’ligand. In addition, the analysis through of 1 H and 13 C NMR spectroscopy, confirm that the synthesis and yield of just one isomer of this compound.