A triclinic modification of 5,5 '-dinitro-2,2 '-dithiodipyridine
Abstract
The asymmetric unit of the title compound, C10H6N4O4S2, contains two independent but similar mol-ecules. The structure is a triclinic polymorph of the monoclinic structure reported previously [Brito, Mundaca, Cárdenas, López-RodrÃguez & Vargas (2007). Acta Cryst. E63, o3351-o3352]. The most obvious difference between the two polymorphs is the C - S - S - C torsion angle [-80.13 (16), -79.8 (2) and 0° for the two mol-ecules of the triclinic polymorph and the monoclinic polymorph, respectively]. The crystal structure of the title compound has two intra-molecular C - H⋯S inter-actions with average H⋯S distances of 2.69 Ã…, whereas this kind of inter-action is not evident in the monoclinic polymorph. © International Union of Crystallography 2008.
Más información
Título según WOS: | A triclinic modification of 5,5 '-dinitro-2,2 '-dithiodipyridine |
Título según SCOPUS: | A triclinic modification of 5,5'-dinitro-2,2'-dithio-dipyridine |
Título de la Revista: | ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE |
Volumen: | 64 |
Número: | 1 |
Editorial: | WILEY-BLACKWELL |
Fecha de publicación: | 2008 |
Página de inicio: | O102 |
Página final: | U3419 |
Idioma: | English |
URL: | http://scripts.iucr.org/cgi-bin/paper?S1600536807062630 |
DOI: |
10.1107/S1600536807062630 |
Notas: | ISI, SCOPUS |