1-(3-Phenylisoxazol-5-yl)cyclohexane-1,2-diol
Abstract
In the title compound, C 15H 17NO 3, there are two mol-ecules in the asymmetric unit wherein the isoxazole rings make dihedral angles of 16.16 (15) and 16.79 (13)° with the benzene rings, and the cyclo-hexane rings adopt chair conformations. In both mol-ecules, the hydroxyl groups of the diol fragments are cis oriented, the O - C - C - O torsion angles being 60.76 (12) and -55.86 (11)°. The two mol-ecules are linked by a strong O - H?N hydrogen bond and the crystal packing is stabilized by one O - H?N and two O - H?O hydrogen bonds. An intra-molecular O - H?O hydrogen bond is observed in one of the molecules.
Más información
Título según WOS: | 1-(3-Phenylisoxazol-5-yl)cyclohexane-1,2-diol |
Título según SCOPUS: | 1-(3-Phenylisoxazol-5-yl)cyclo-hexane-1,2-diol |
Título de la Revista: | ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE |
Volumen: | 65 |
Número: | 7 |
Editorial: | WILEY-BLACKWELL |
Fecha de publicación: | 2009 |
Página de inicio: | O1509 |
Página final: | U1917 |
Idioma: | English |
URL: | http://scripts.iucr.org/cgi-bin/paper?S1600536809020947 |
DOI: |
10.1107/S1600536809020947 |
Notas: | ISI, SCOPUS |