1-(3-Phenylisoxazol-5-yl)cyclohexane-1,2-diol

Astudillo, L; Brito, I; Vallejos G.; Gutiérrez M; Lopez-Rodriguez, M

Abstract

In the title compound, C 15H 17NO 3, there are two mol-ecules in the asymmetric unit wherein the isoxazole rings make dihedral angles of 16.16 (15) and 16.79 (13)° with the benzene rings, and the cyclo-hexane rings adopt chair conformations. In both mol-ecules, the hydroxyl groups of the diol fragments are cis oriented, the O - C - C - O torsion angles being 60.76 (12) and -55.86 (11)°. The two mol-ecules are linked by a strong O - H?N hydrogen bond and the crystal packing is stabilized by one O - H?N and two O - H?O hydrogen bonds. An intra-molecular O - H?O hydrogen bond is observed in one of the molecules.

Más información

Título según WOS: 1-(3-Phenylisoxazol-5-yl)cyclohexane-1,2-diol
Título según SCOPUS: 1-(3-Phenylisoxazol-5-yl)cyclo-hexane-1,2-diol
Título de la Revista: ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
Volumen: 65
Número: 7
Editorial: WILEY-BLACKWELL
Fecha de publicación: 2009
Página de inicio: O1509
Página final: U1917
Idioma: English
URL: http://scripts.iucr.org/cgi-bin/paper?S1600536809020947
DOI:

10.1107/S1600536809020947

Notas: ISI, SCOPUS