Microwave-assisted synthesis and regioisomeric structural elucidation of novel benzimidazo[1,2d][1,4]benzodiazepinone derivatives
Abstract
The synthesis of 5H-benzimidazo [1,2-d] [1,4] benzodiazepin-6(7H)-ones 3a-e from readily available 2-(2-aminophenyl)-1H-benzo[d]imidazole derivatives 2a-e and 2-bromoacetyl bromide under microwave conditions is described. Unambiguous structural elucidation of the obtained regioisomers was finally established by means of 2D-NOESY experiment. © ARKAT USA, Inc.
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Título según WOS: | Microwave-assisted synthesis and regioisomeric structural elucidation of novel benzimidazo[1,2d][1,4]benzodiazepinone derivatives |
Título según SCOPUS: | Microwave-assisted synthesis and regioisomeric structural elucidation of novel benzimidazo[1,2d][1,4]benzodiazepinone derivatives |
Título de la Revista: | ARKIVOC |
Volumen: | 2009 |
Número: | 12 |
Editorial: | ARKAT USA INC |
Fecha de publicación: | 2009 |
Página de inicio: | 131 |
Página final: | 140 |
Idioma: | eng |
Notas: | ISI, SCOPUS |