Crystal structure and spectroscopic data of fac-tricarbonylbromo(3,3?-trimethylene-2,2?-bi-1,8-naphthyridine) rhenium(I), Re(CO) 3Br(C 19H 14N 4)

MOYA, S. A.; Schmidt, R; Pastene, R.; Sartori R.; Muller, U; Frenzen G.

Abstract

The title compound 1 was obtained from Re(CO) 5Br and the binaphthyridine in heptane. Its X-ray crystal structure determination shows a molecular structure with the two nitrogen atoms in positions 1 and 1? acting as a bidentate chelate ligand to the Re atom. 1H NMR, UV-vis, and IR spectroscopic data are reported and assigned.

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Título de la Revista: ORGANOMETALLICS
Volumen: 15
Número: 15
Editorial: AMER CHEMICAL SOC
Fecha de publicación: 1996
Página de inicio: 3463
Página final: 3465
URL: http://www.scopus.com/inward/record.url?eid=2-s2.0-0000732712&partnerID=q2rCbXpz